Laboratory Analysis Techniques for Soil, Organic Waste, Compost and Food Characterization.
Keywords:
suelo, muestras de compost, biomasa, residuos orgánicos, contaminaciónSynopsis
Inadequate management of organic solid waste from the agro-industrial sector has led to the contamination of natural resources, especially on the ground. The composting process is an environmentally friendly ecotechnology, its final product is the compost used as an organic amendment in the agricultural sector. For the implementation of this treatment system, it is important to characterize the physical-chemical, chemical and biological soils, residues, compost as well as those foods produced as raw material for the agro-industrial sector. On the other hand, the numerous analysis techniques that are used in various laboratories in the country make it necessary to have reliable analytical techniques that guarantee reliability in the results obtained, so the objective of this document is the detailed description of laboratory analysis techniques. for the characterization of soil samples, organic waste, compost and food with the purpose of guaranteeing quality in the results. For this, laboratory analysis techniques have been compiled that have been validated and standardized according to current norms, regulations and investigations that will allow obtaining reliable results when implemented in other laboratories. The techniques presented will be developed from the characterization of soils, organic waste, compost and food, including the preparation of samples, the determination of physical and chemical parameters, and the interpretation of the results.
Keywords: soil, compost samples, biomass, organic waste, contamination
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Ambiente, C. D. E. M., & De La Junta, D. E. A. (1999). Los Criterios Y Estándares Para Declarar Un Suelo Contaminado En Andalucía Y La Metodología Y Técnicas De Toma De Muestra Y Análisis Para Su Investigación.
-P Phosphorus - Standard Methods For The Examination Of Water And Wastewater, Standard Methods For The Examination Of Water And Wastewater, 23rd. (2018). Https://Www.Standardmethods.Org/Doi/10.2105/Smww.2882.093
Astm-D-2216-19. (2019). Standard Test Method For Laboratory Determination Of Water (Moisture) Content Of Soil And Rock By Mass. Astm International, January, 1-5. Https://Www.Astm.Org/D2216-19.Html
Astm D1193-06. (2011). Standard Specification For Reagent Water. En Astm International. Https://Www.Astm.Org/D1193-99.Html
Astm D2974. (2020). Standard Test Methods For Determining The Water (Moisture) Content, Ash Content, And Organic Material Of Peat And Other Organic Soils. Astm International, 1-4. Https://Www.Astm.Org/D2974-20e01.Html
Chávez-Ramos, K., & Bonilla-Martínez, D. (2014). La Formación De Precipitados Bajo El Efecto De La Acidez En El Método De Mohr. Educación Química, 25(4), 440-445. Http://Www.Scielo.Org.Mx/Scielo.Php?Script=Sci_Arttext&Pid=S0187-893x2014000400006&Lng=Es&Nrm=Iso&Tlng=Es
Chemists., A. Of O. A. (2023a). Aoac 934.01-1934, Loss On Drying (Moisture) At 95°C-100°C For Feed - Aoac Official Method. Http://Www.Aoacofficialmethod.Org/Index.Php?Main_Page=Product_Info&Products_Id=671
Chemists., A. Of O. A. (2023b). Aoac 978.04-1978, Nitrogen (Total) (Crude Protein) In Plants. : Aoac Official Method. Http://Www.Aoacofficialmethod.Org/Index.Php?Main_Page=Product_Info&Cpath=1&Products_Id=1116
Composting Counsil. (S. F.). Test Methods For The Examination Of Composting And Compost. Https://Www.Compostingcouncil.Org/Page/Tmecc?&Hhsearchterms=%22tmecc%22
Csuros, M., & Csuros, C. (2016). Environmental Sampling And Analysis For Metals. Crc Press.
Epa, U. S. (2019). U.S. Epa Method 3051a: Microwave Assisted Acid Digestion Of Sediments, Sludges, And Oils. En Us Epa. Https://Www.Epa.Gov/Hw-Sw846/Sw-846-Test-Method-3051a-Microwave-Assisted-Acid-Digestion-Sediments-Sludges-Soils-And
Flores Delgadillo, L., & Alcalá Martínez, J. R. (2010). Manual De Procedimientos Analíticos. Física De Suelos. Https://Docplayer.Es/6383660-Manual-De-Procedimientos-Analiticos-Fisica-De-Suelos.Html
Folin, O., & Ciocalteu, V. (1927). On Tyrosine And Tryptophane Determinations In Proteins. Journal Of Biological Chemistry, 73(2), 627-650. Https://Doi.Org/10.1016/S0021-9258(18)84277-6
Hach, C. (2000). Manual De Análisis De Agua. Loveland, Colorado, Ee. Uu.
Henríquez, M., Pérez, J., Gascó, J. M., & Rodríguez, O. (2005). Determinación De La Capacidad De Intercambio Catiónico En Arena Y Caolín Usando Acetato De Amonio, Acetato De Sodio Y Cloruro De Amonio. Bioagro, 17(1), 59-62. Http://Ve.Scielo.Org/Scielo.Php?Script=Sci_Arttext&Pid=S1316-33612005000100008&Lng=Es&Nrm=Iso&Tlng=Es
Hernando, C., & Rengifo, A. (1974). Comparacion De Cinco Metodos Para Determinar Capacidad De Intercambio Cationico En Suelos Alcalinos. Acta Agronómica, 24(1-4), 66-92. Https://Doi.Org/10.15446/Acag
Iso. (1995). Soil Quality. Determination Of Total Nitrogen - Modified Kjeldahl Method. Iso 11261:1995. 1995, 4. Https://Www.Iso.Org/Standard/19239.Html
Iso 11265:1994 - Soil Quality — Determination Of The Specific Electrical Conductivity. (S. F.). Recuperado 5 De Abril De 2023, De Https://Www.Iso.Org/Standard/19243.Html
Ministerio Del Ambiente. (2015). Acuerdo Ministerial 097a-Edición Especial No. 387. 1-184. Https://Www.Registroficial.Gob.Ec/Index.Php/Registro-Oficial-Web/Publicaciones/Ediciones-Especiales/Item/5550-Edición-Especial-No-387
Normalización Española. (2001). Une-En 13342:2001 Caracterización De Lodos. Determinación Del ... Https://Www.Une.Org/Encuentra-Tu-Norma/Busca-Tu-Norma/Norma?C=N0024735
Organización De Las Naciones Unidas. (2019). Definiciones | Portal De Suelos De La Fao | Organización De Las Naciones Unidas Para La Alimentación Y La Agricultura. 2019. Https://Www.Fao.Org/Soils-Portal/Soil-Survey/Clasificacion-De-Suelos/Sistemas-Numericos/Propiedades-Quimicas/Es/
Osorio, W., & Casamitjana, M. (2012). Toma De Muestras De Suelo Para Evaluar La Fertilidad Del Suelo. Manejo Integral Del Suelo Y Nutrición Vegetal, 1(1), 23-28.
Radojevic, M., Bashkin, V., & Bashkin, V. N. (2006). Practical Environmental Analysis. Royal Society Of Chemistry.
Rodríguez, O., & Rodríguez, A. (2002). Comparación De La Cic En Dos Suelos, Utilizando Acetato De Amonio, Acetato De Sodio Y Cloruro De Amonio. Revista De La Facultad De Agronomía, 19(4), 253-263. Http://Ve.Scielo.Org/Scielo.Php?Script=Sci_Arttext&Pid=S0378-78182002000400001&Lng=Es&Nrm=Iso&Tlng=Es
Skoog, D. A., Holler, F. J., & Nieman, T. A. (2018). Principios De Análisis Instrumental. Mcgraw-Hill Madrid.
Soil Sampling | Us Epa. (2020). Us Epa. Https://Www.Epa.Gov/Quality/Soil-Sampling
Standard Methods. (2011). 1060 Collection And Preservation Of Samples - Standard Methods For The Examination Of Water And Wastewater. 1060. Https://Www.Standardmethods.Org/Doi/10.2105/Smww.2882.009
Standarization, I. O. For. (2002). Iso 10381-2: Soil Quality-Sampling. Part 2: Guidance On Sampling Techniques. International Organization For Standardization Geneva.
Sw-846 Test Method 9045d: Soil And Waste Ph | Us Epa. (2004). Https://Www.Epa.Gov/Hw-Sw846/Sw-846-Test-Method-9045d-Soil-And-Waste-Ph
Technologies, T. (2019). Icp Glossary Of Terms. Https://Www.Teledyneleemanlabs.Com/Resource/Documents/Icp Glossary Of Terms.Pdf
Thiex, N., Novotny, L., & Crawford, A. (2012). Determination Of Ash In Animal Feed: Aoac Official Method 942.05 Revisited. En Journal Of Aoac International (Vol. 95, Número 5, Pp. 1392-1397). Oxford Academic. Https://Doi.Org/10.5740/Jaoacint.12-129
United States Environmental Protection Agency. (2007). Sw-846 Test Method 7000b: Flame Atomic Absorption Spectrophotometry. Https://Www.Epa.Gov/Hw-Sw846/Sw-846-Test-Method-7000b-Flame-Atomic-Absorption-Spectrophotometry
Usepa. (2014). Chapter Three Of The Sw-846 Compendium. Https://Www.Epa.Gov/Hw-Sw846/Chapter-Three-Sw-846-Compendium-Inorganic-Analytes
Usepa (United States Environmental Protection Agency). (1996). Epa Method 3050b Acid Digestion Of Sediments, Sludges And Soils, Sw-846 Revision 2. October, 2012. Https://Www.Epa.Gov/Esam/Epa-Method-3050b-Acid-Digestion-Sediments-Sludges-And-Soils
Walkley, A., & Black, I. A. (1934). An Examination Of The Degtjareff Method For Determining Soil Organic Matter, And A Proposed Modification Of The Chromic Acid Titration Method. Soil Science, 37(1). Https://Journals.Lww.Com/Soilsci/Fulltext/1934/01000/An_Examination_Of_The_Degtjareff_Method_For.3.Aspx
Zucconi, F. And De Bertoldi, M. (1987) Compost Specifications For The Production And Characterization Of Compost From Municipal Solid Waste. In De Bertoldi, M., Ferranti, M.P., L′Hermite, M.P. And Zucconi, F., Eds., Compost Production, Quality And Use, El. (S. F.). Recuperado 11 De Mayo De 2023, De Https://Www.Scirp.Org/(S(Lz5mqp453edsnp55rrgjct55))/Reference/Referencespapers.Aspx?Referenceid=1463430
Zucconi, F. (1981). Evaluating Toxicity Of Immature Compost. Biocycle, 22(2), 54-57.
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